MS Report from Instrument: HY-LCMS-02 File ..M32\\1\\DATA\\20170221\\CPK\\CPK2017-221-11575.D Tgt Mass (EZX): 545.54 Injection Date : 21 Feb 17 4:58 pm +0800 Seq. Line : 0 Sample Name : CPK2017-221-11575 Location : P2-F-04 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-13897 Batch#11575 Easy-Access Method: '1-POS-3MIN' 545.54 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU150010001.2441.2721.3901.4921.63950000.5*DAD1 C, Sig=254,4 Ref=off mAU10001.2091.25950000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 702000001500001000005000001.31811.3131.7131.3131.522.5min*1.3971.4921.5701.6391.7141.522.5min*1.4030.511.5 Ion 546.54, MSD1 546.54,Target Mass 545.54 +H Positive, EIC=546.24:547.24 60000400002000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.51.3161.35022.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.24 0.02 1.87 1.90 0.06 ND 1.27 0.01 2.35 2.73 0.07 274 1.31 0.03 3324.68 2010.03 98.06 274 1.39 0.02 11.83 8.26 0.35 274 1.49 0.03 20.99 13.28 0.62 546 1.64 0.02 5.84 3.93 0.17 141 1.71 0.03 22.86 0.44 0.67 141 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.04 2.28 -0.06 0.09 ND 1.26 0.02 3.36 0.98 0.14 274 1.31 0.03 2374.59 1445.04 98.52 274 1.40 0.03 12.00 7.53 0.50 274 1.49 0.03 12.72 8.00 0.53 546 1.57 0.02 1.02 0.94 0.04 ND 1.64 0.02 3.05 2.22 0.13 141HY-LCMS-02 2/22/2017 9:51:56 AM GZZ_718Page 1 of 3
MS Report from Instrument: HY-LCMS-02
1.71 0.03 1.25 0.04 0.05 141HY-LCMS-02 2/22/2017 9:51:56 AM GZZ_718Page 2 of 3
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.32 <<<< POSITIVE SPECTRA >>>> ES-API Positive50000400003000020000100000200 273.7 547.2 546.3 568.2300400500600700800m/zRet. Time: 1.40 ES-API Positive 273.7500040003000200010000200 141.1 560.2 584.0 233.1 547.2 546.2 445.3 718.0300400500600700800900m/zHY-LCMS-02 2/22/2017 9:51:56 AM GZZ_718Page 3 of 3